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  • Central Research Instrumentation Facility (CRIF) Facilities People Tariff Upcoming Facilities Annual Expenditure and Revenue Contact Us Events Requisition Forms

    Central Research Instrumentation Facility (CRIF)



     

     

    About CRIF

    Central Research Instrumentation Facility (CRIF) is an integrated facility to provide high-end analytical services to academic and industrial research. The CRIF works with a motto to bring out the research output of scholars matching the international standards. The central facility caters to the department requirements under a single umbrella by fostering interdisciplinary research. Students from the different branches of science and engineering come here for research and experimentation, creating a vibrant cross-disciplinary atmosphere. The CRIF is committed to expanding to facilitate state-of-the-art laboratory services to all academia and industries located across the country. The facility is spread across in an area of 19000 sq. ft.


    Facilities



    Liquid Chromatography-High Resolution Mass Spectrometry (LC-HRMS)

     

    Make:Agilent Technologies

    Model: QTOF 6530

    Cost :1,22,87,540.00


    Applications:The molecular structure of petroleum components, industrial products, pharmaceuticals and biomolecules can be judged. The purity of the finished chemical industrial products is established.


    Specifications:

    MASS Spectrometer

    • Mass Range m/z 100-20000 High mass range

    m/z 50-3200 High-resolution mode
     

    • Sensitivity (1 pg. Reserpine signal noise ratio >180:1)
       
    • Mass Accuracy <2ppm
       
    • Resolution (FWHM) 20000
       
    • Ionization Method: ESI & APCI

    1) ESI positive & negative 2) APCI positive & negative
     

    LC  SYSTEM

    • Pump:1290 infinity quaternary pump with 1200 bar maximum pressure
       
    • Detector:1260 infinity Diode array detector(DAD)190-950nm
       
    • Flow rate:0.001-5ml/min

     


    X Band ESR Spectroscopy

     

    MakeJEOL  RESONANCE Inc., Japan

    Model:JES-FA100

    Cost :97,19,783.00


    Applications: ESR Spectrometer is used for the measurement of species that contain unpaired electrons (Free radicals, transition metal complexes, molecular structure, valence electron wave functions, electron transport, crystal & ligand field splitting, relaxation mechanisms and reaction kinetics, odd-electron molecules, rare earth ions etc. ESR is a powerful non-destructive and non-intrusive analytical method. ESR yields meaningful structural information even from ongoing chemical or physical processes, without influencing the process itself.


    Specifications:

    • Standard Frequency (X band) - 8.75-9.65 GHz
       
    • Sensitivity - 7x109 spins/0.6mT
       
    • Resolution – 3 μT or better-Temperature study - Variable Temperature facility (-153 to +25 °C)



    Inductively Coupled Plasma Optical-Emission spectroscopy

    Make: Agilent Technologies

    Model: 700 series

    Cost :27,58,005.00


    Applications: This technique is used for quantitative and qualitative determination of the metals and metalloids in the following sample.

    1. Biological
       
    2. Environmental
       
    3. Pharmaceutical
       
    4. Industrial
       
    5. Aqueous and Organic


    Specifications:
     

    Plasma Generator

    • RF Generator: Solid-state generator with quick (<1 hour) warm-up
       
    • Frequency: 27.12 MHz or higher
       
    • Power: Up to 1500 watts (computer-adjustable)
       
    • Controls: Fully computer-controlled and software-driven
       
    • Argon: Argon flow rates monitored
       
    • Plasma Detection: Plasma should be radially viewed / or axially viewed/ or dually viewed (through protective screens)
       
    • Chiller: Internal (by Peltier) or External along with equipment for RF coil cooling


    Optical System

    • Wavelength range: 170to 770 mm wider
       
    • Focal length: more than 0.5 meters for holographic grating/More than 0.32 meter for Echelle grating
       
    • Optical Resolution:
      • Better than 10 pm in the UV range (below 300 nm)
      • Better than 17 pm in the visible range (above 350nm)
         

    UV purge: Nitrogen/argon pure/gas sealed for 165 to 190nm please specify the gas consumption during the analytical flow (considering UV elements), standby and shutdown mode.

     

    UV-Vis NIR Spectrophotometer

     

    Make: Agilent Technologies

    Model: Carry 5000

    Cost :39,49,816.00


    Applications: The electronic transitions and band gaps of semiconductors, thin films, etc. can be determined. Electronic structures of polymers, complexes, biomolecules, materials, pharmaceuticals and other products can be evaluated.


    Specifications:

    • Photometric System: Double Beam, Double Monochromatic
       
    • Wavelength Range: 3300 to 175 nm (+)
       
    • Bandwidth: 0.01 and 0.04 nm (+)
       
    • Resolution: 0.048 and 0.2 nm (+)

     

    Flouresence Workstation

    Make: HORIBA INSTRUMENTS INCORPORATED, USA

    Model: FL-1000

    Cost :74,48,136.00


    Applications: Molecular and solid-state fluorescence emission can be monitored and quantum lifetime measurements can be evaluated. Materials in all states and biological samples can be investigated.


    Specifications:

    • Excitation & Emission Wavelength Range: 200nm – 1000nm
       
    • Wavelength Accuracy: 0.5

     

    Universal Testing Machine (UTM)

     

    Make: JINAN TESTING EQUIPMENT IE CORPORATION, China

    Model: WDW-100S

    Cost :61,93,158.00


    Applications: It can perform many standard tensile and compression tests on materials, components and structures. Physical and mechanical attributes of metals, alloys, finished solid products, etc., can be studied. Aforesaid tests can also be performed under sub-zero (-100C) and high-temperature (up to 1000C) conditions.


    Specifications:

    • Maximum Load : ± 100kN
       
    • Temperature : -1000C to 3000C (chamber)

                                3000C to 10000C (3-Zone split furnace)
     

    • Available extensometers: 25mm, Resolution=0.1μm (15% maximum strain)

                                                   12.5mm. Resolution=0.1μm
     

    • Day Light: 1400 mm
       
    • Speed range: 0.0005 mm/min to 500mm/min

     

     

    Trinocular Polarizing Microscope

    Make: Olympus

    Model: BX53

    Cost :12,43,448.00


    Applications: Trinocular Polarizing Upright Research Microscope withInfinity corrected optical system. External power supply. Coaxialcoarse and fine focussing 1 micron, with torque adjustable focusstopper with built-in filter cassettes (NCB filter, Blue and otherconversion filters)


    Specifications:

    Transmitted Illumination:12v 100w halogen external with power supply 12v 100w lamp halogen lamp 12v 100w (2Nos).

    Polarizer: Intermediate tube with 360deg rotatable polarizer for transmitted light fitted below the condenser with a swing in the swing-out facility.

    Eye Piece tube: Three-way trinocular eyepiece tube 100/0,0/100,20/80 or 50/50 light distribution.

    Eyepiece Type: 10*eyepiece with 22 mm or better field of view and dioptre adjustment on both eyepiece and one-piece with a crosshair.

     

    NMR Spectroscopy

    Make: Bruker

    Model: Ascend 400 MHz

    Cost :1,85,00,00


    Applications: Molecular Structure Determination of

    Condenser: Achromatic strain-free condenser N.A0.90with iris diaphragm. Compensator: Quartz wedge lambda tint plate and bedeck.

    Reflected illuminated: Attached with halogen illumination lamp 100w halogen illuminated with external power supply incident light polarizer 360degrotatable analyser with filler Organic compounds, Pharmaceuticals and Drugs. Structure and atomic arrangements in molecules and crystals can be investigated. Kinetic and temperature studies of reaction mixtures.   

    1D-NMR: 1H, 13C, 31P, 19F, DEPT-135, DEPT-90, DEPT-45,1D_NOESY,Water Suppression, VT Temperature

    2D-NMR:   *HOMO: NOESY, COSY, TOCSY

    *HETERO: HSQC, HMBC


    Specifications:

    • UltraShieldTM Plus 9.4T magnet
       
    • 5 mm BBFOPLUS probe, optimized for X-nuclei direct observation. Broadband in a frequency range between 31P and 15N. This probe has 2H "lock" channel and z gradient that allows us to carry out 2D spectroscopy and hetero correlation 19F/1H and 1H/19F.
       
    • Control temperature unit (from -50 °C to 50 °C).

     

    Scanning Electron Microscope (SEM)

    Make: TESCAN

    Model: VEGA3 LMU

    Cost :1,00,00,000


    Applications: Surface Studies, Nano Particle imaging, Phase transitions, Corrosion products and all kinds of solid material studies.


    Specifications:

    • Electron Gun: Tungsten heated cathode / optionally LaB6
       

     Resolution: 1 μm in the secondary electron mode at a working distance of 5 mm

    X-Ray Diffraction (XRD)

    Make: Panalytical

    Model: X-pert powder

    Cost :1,00,00,000


    Applications: Powder XRD equipment can be used for the characterization of powder samples for the phase analysis, Identifying crystalline phases and orientation and crystallographic information. This equipment can also capture data from the bulk polycrystalline samples after the required sample preparation. Structural properties such as Lattice parameters, Strain, Grain size, texture and epitaxy can be determined from the data. The XRD diffraction data will be provided to the user and the user can investigate the above materials' properties by analysing the data.


    Specifications:

    • Source: Cu target X-Ray tube
       
    • X-Ray Power: 2KW
       
    • Operation Modes: Vertical & Horizontal
       
    • Accuracy: ±0.0025
       
    • 2º θ Measurement range: 60 to130º
       
    • Diffractometer radius: 130 to 230 mm
       
    • Radiation: Cu Kα;
       
    • Software: X’perthighscore plus

     


    TGDTA

    Make: Netzsch

    Model: Regulars STA 2500

    Cost :22,79,273.62


    Applications: High-performance analytical instruments by NETZSCH Analysing & Testing allow for comprehensive analysis of the thermal properties of a great variety of materials. Select the appropriate testing methods for your polymers and other organic materials, metals and alloys, ceramics, glass, building materials or other inorganic materials from among our various series of instruments.


    Specifications:

    • Temp. range: RT to 1700oC
       
    • Heating Rate: 0.1o-100oC/min.
       
    • Weight:10mg to 40mg
       
    • Atmosphere: Argon, Nitrogen
       
    • Purge gas flow:50,
       
    • Protective gas flow: 20
       
    • Sample capacity(Max): 200mg
       
    • Pans:30micro litre


    Impedance Analyser

    Make: Biologic

    Model: MTZ35

    Cost :31,81,094.45


    Applications: : Impedance analysers are often used for characterization of many electrochemical devices, such as photovoltaic cells, fuel cells and batteries that are commonly utilized in renewable energy applications. Depending upon the specifications of these devices, they are quite expensive and their use in many low-cost applications is limited. This study demonstrates a practical impedance analyser application based on the cross-correlation method. Some techniques for extending the bandwidth of the analyser and smoothing out the frequency response are presented. The theoretical studies are verified on a digitally controlled boost converter that identifies a second-order impedance network


    Specifications:

    Temp:1100c

    Frequency range:10-35MHz

    Accuracy:0.05

    Insulation material: Alumina Fibre

    Heating System: Super Kanthal 1350°C wire built in a cement cylinder

    Temperature Range: Ambient up to 1100°C

    Temperature Controller: PM6 Walton PID controller

    Temperature Sensors: K-Type Thermocouple

    Temperature Control Accuracy: Better than +/-1°C

    Temperature scan: adjustable (from 0.1 °C/min to 20 °C/min)

    Safety Features: Emergency stop button; Buzzer sound alarm; Temperature safety limit


    18000C Furnace

    Make: Nabertherm

    Model: LTH02/16

    Cost :10,75,647.00

    Specification: Max temp:1800c

    Chamber dimentions:90*150*150mm

    Chamber volume: 2lit

    Power rating:3.0

    Adjustable air inlet

    Type B thermocouple

    Max programs: 9 Steps


    Electrochemical Workstation

    Make: ZAHNER

    Model:IM6e

    Cost :14,36,575.00

    Specifications:

    Frequency Range DC-1MHz

    ADC/DAC resolution 16 bit

    Shell Ground

    Harmonic reject >60dB@ 0.5 full scale

    Dimensions 364 x 160 x376 mm * Weight 12 Kg

     

    Vacuum Arc Melting
     

    Make: VEC Solutions

    Cost :8,61,343.00


    Specifications:

    • Fast response time
       
    • Covering range from 0.5mb to 10-3 mbar
       
    • Rugged construction of sensors
       
    • Single gauge head for entire measuring range
       
    • Metal G.H with standard KF-10 coupling
       
    • Measuring range: 0.5mbar 1x10-3mbar  
       
    • Mode: Analog
       
    • Tolerance (Accuracy):20 %
       
    • Power Supply : 230V Ac single phase 50 Hz
       
    • G.H. Connection: KF-10
       
    • Response Time: about 1 sec
       
    • Principle: Thermal Conductivity
       

    Output: 0 to 100 mV DC at fsd used for controller

     

    Differential Scanning Calorimeter

    Make:PerkinElmer

    Model:DSC8000

    Specifications:

    Range -180 C to 750 C

    Accuracy ±0.05 C Using on-set temperatures of Indium melting peak

    Precision ±0.008 C

    Data points/sec 33

    Controlled heating rates 0.01 to 300 C/min

    Controlled cooling rates 0.01 to 150 C/min

    Controlled Cooling Ambient coolant – nitrogen purge

    10 C/min to 22 C

    20 C/min to 35 C

    50 C/min to 70 C

    100 C/min to 125 C

     

    17000C Furnace/16000C Furnace

     


    Make: OKAY

    Model: LTH02/16

    Specification: Max temp:1700c

    Heating element Mo, Disilicide,

    Heating Space:150w*150 H*150mm

    Segments:16

    Condenser: Achromatic strain-free condenser N.A0.90with iris diaphragm.

    Compensator: Quartz wedge lambda tint plate and bedeck.

     


    People



    CRIF TEAM
     

    1. Dr. T Krishna Sai, Principal Scientific Officer
     

    2. Shri V Sudhakar, Technical Officer
     

    3. Shri M Harish, Technical Officer
     

    4. Shri D Ravikumar, Technical Officer
     

    5. Smt GSR Sanjeevini, Technical Officer
     

    Mail ID:  techofficer_crif@nitw.ac.in
     

    Landline Phone No : +91 870 2462966-2965            

     


    Tariff




    Upcoming Facilities



     

    A laboratory setup for Antenna design is formed at CRIF. Purchase order for procurement of Anechoic Chamber, Vector Network Analyser, Spectrum Analyser and PCB Prototype are in Place. The set up will become operational in April, 2022.


    Annual Expenditure and Revenue




    Contact Us



     

    Mail ID:  techofficer_crif@nitw.ac.in

    Landline Phone No : +91 870 2462966-2965            


    Events



     

    • 29 Apr 2022 :  Call for registrations for "One-week training program on R&D Equipment " (27th May-02nd June 2022) under DST funded STUTI-21 Project organized by CRIF, NITW (Rescheduled) (Deadline extended till 18th May 2022 6 PM)   
       
    • 05 Apr 2022 : Call for registrations for "One-week training program on R&D Equipment at JNTUH" (18th-24th April 2022) under DST funded STUTI-21 Project organized by CRIF, NITW & JNTU Hyderabad   (Completed)
       
    • 22 Mar 2022 : Call for Registration for One Week Training Program on R&D Equipment under DST funded STUTI-21 project (4th -10th April 2022) organized by CRIF,NITW   (Completed)

    Requisition Forms



    • User Requisition Form for CD-ORD
       
    • User Requisition Form for NMR Spectrometer
       
    • User Requisition Form for ESR Spectrometer
       
    • User Requisition Form for ICP-OES
       
    • User Requisition Form for Impedance Analyzer
       
    • User Requisition Form for LCHRMS
       
    • User Requisition Form for Universal Testing Machine (UTM)
       
    • User Requisition Form for UV Vis NIR Spectrometer
       
    • User Requisition Form for Vacuum Arc Re-melting Furnace (VARF)
       
    • User Requisition Form for DSC
       
    • User Requisition Form for FURNACE
       
    • User Requisition Form for TGDTA
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